4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

Base Information

Chemical Name:4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate
CAS No.:80898-80-2
Molecular Formula:C₁₃H₁₀N₂O₅S₂
Molecular Weight:338.365
Hs Code.:

Synonyms:4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

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Chemical Property of 4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

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Technology Process of 4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

There total 9 articles about 4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 80909-65-5
(2-Chloro-4-oxo-azetidin-1-yl)-(4-oxo-[1,3]dithietan-2-ylidene)-acetic acid 4-nitro-benzyl ester

: 80898-80-2
4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: With methylamine; In methanol; at 0 ℃;
DOI:10.1039/c39820000713

Reference yield: 48.0%

: 123-91-1,28347-88-8,28347-91-3,39449-24-6,54841-74-6
1,4-dioxane

: 288-32-4
1H-imidazole

: 83362-40-7
4-nitrobenzyl 3-acetylthio-7-oxo-4-thia-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

: 80898-80-2
4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: In water;

Reference yield:

: C₁₄H₁₂N₂O₅S₃^(2-)*2Li⁽¹⁺⁾

: 80898-80-2
4-Nitrobenzyl 7-oxo-3-thioxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / tetrahydrofuran / -78 °C

2: Cl₂ or SO₂Cl₂ / CH₂Cl₂ / 0 °C

3: 63 percent / MeNH₂ / methanol / 0 °C

With chlorine; methylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c39820000713