N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine

Base Information

• Chemical Name: N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine
• CAS No.: 1097907-11-3
• Molecular Formula: C₁₉H₂₆N₆O
• Molecular Weight: 354.455

Synonyms:N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine

Chemical Property of N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine

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Technology Process of N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine

There total 1 articles about N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(2-hydroxybenzyl)-N,N'-bis[2-(N-methylimidazolyl)methyl]imidazolidine → N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine (1097907-11-3)

Guidance literature:

With sodium cyanoborohydride; trifluoroacetic acid; In ethanol; for 2h;

DOI:10.1002/ejic.200601236

Reference yield: 26.0%

N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine (1097907-11-3) + 2-(1-(6-hexanal)-1H-1,2,3-triazol-4-yl)pyridine chlorotricarbonylrhenium → C35H42ClN10O4Re

Guidance literature:

N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine; 2-(1-(6-hexanal)-1H-1,2,3-triazol-4-yl)pyridine chlorotricarbonylrhenium; With triethylamine; In ethanol; Inert atmosphere;

With sodium cyanoborohydride; trifluoroacetic acid; In ethanol; Inert atmosphere;

DOI:10.1039/d0cc03398g

Reference yield: 25.0%

N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine (1097907-11-3) + glycine (56-40-6,18875-39-3,25718-94-9) + trifluoroacetic acid (76-05-1) + Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine (187618-60-6) → C23H32N8O3*4C2HF3O2

Guidance literature:

Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; for 2h;

With piperidine; In 1-methyl-pyrrolidin-2-one;

N-(2-hydroxybenzyl)-N,N′-bis[2-(N-methylimidazolyl)methyl]ethane-1,2-diamine; glycine; trifluoroacetic acid; Further stages;

DOI:10.1016/j.jinorgbio.2016.01.025

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