4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate

Base Information

Chemical Name:4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate
CAS No.:957855-47-9
Molecular Formula:C₂₈H₄₁N₅O₃
Molecular Weight:495.665
Hs Code.:

Synonyms:4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate

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Chemical Property of 4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate

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Technology Process of 4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate

There total 4 articles about 4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 957855-48-0
4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6-oxo-7H-pteridin-2-yl]amino]-3-methoxy-benzoate

: 957855-47-9
4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate

Guidance literature:: 4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6-oxo-7H-pteridin-2-yl]amino]-3-methoxy-benzoate; With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; for 5h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 16h;

With ammonia; In methanol;

Reference yield:

: 41608-64-4
methyl 3-methoxy-4-aminobenzoate

: 957855-47-9
4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / 5 h / Heating / reflux

2.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 20 °C

2.2: 16 h / 20 °C

With dimethylsulfide borane complex; toluene-4-sulfonic acid; In tetrahydrofuran;

Reference yield:

: 108-11-2,72847-31-5
Methyl isobutyl carbinol

: 957855-47-9
4-methylpentan-(2R/S)-yl 4-[[(7R)-8-cyclopentyl-7-ethyl-5-methyl-6,7-dihydropteridin-2-yl]amino]-3-methoxy-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / 5 h / Heating / reflux

2.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 20 °C

2.2: 16 h / 20 °C

With dimethylsulfide borane complex; toluene-4-sulfonic acid; In tetrahydrofuran;