(2S)-2-hydroxy-3-mesitylsulfonyloxypropyl tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:(2S)-2-hydroxy-3-mesitylsulfonyloxypropyl tetra-O-acetyl-β-D-glucopyranoside
CAS No.:130678-85-2
Molecular Formula:C₂₆H₃₆O₁₄S
Molecular Weight:604.629
Hs Code.:

Synonyms:(2S)-2-hydroxy-3-mesitylsulfonyloxypropyl tetra-O-acetyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-2-hydroxy-3-mesitylsulfonyloxypropyl tetra-O-acetyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of (2S)-2-hydroxy-3-mesitylsulfonyloxypropyl tetra-O-acetyl-β-D-glucopyranoside

There total 2 articles about (2S)-2-hydroxy-3-mesitylsulfonyloxypropyl tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 34382-11-1
(2R)-1-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol

: 130678-85-2
(2S)-2-hydroxy-3-mesitylsulfonyloxypropyl tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at -20 ℃; for 168h;
DOI:10.1071/CH9901391

Reference yield:

: 34382-09-7
<(4S)-2,2-dimethyl-1,3-dioxolan-4-yl>methyl tetra-O-acetyl-β-D-glucopyranoside

: 130678-85-2
(2S)-2-hydroxy-3-mesitylsulfonyloxypropyl tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridinium p-toluenesulfonate / methanol / 4 h / Heating

2: 58 percent / pyridine / CH₂Cl₂ / 168 h / -20 °C

With pyridine; pyridinium p-toluenesulfonate; In methanol; dichloromethane;
DOI:10.1071/CH9901391