erythro-3-aminohexestrol 4,4'-dimethyl ether

Base Information

• Chemical Name: erythro-3-aminohexestrol 4,4'-dimethyl ether
• CAS No.: 74536-56-4
• Molecular Formula: C₂₀H₂₇NO₂
• Molecular Weight: 313.44

Synonyms:erythro-3-aminohexestrol 4,4'-dimethyl ether

Chemical Property of erythro-3-aminohexestrol 4,4'-dimethyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of erythro-3-aminohexestrol 4,4'-dimethyl ether

There total 3 articles about erythro-3-aminohexestrol 4,4'-dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

erythro-3-nitrohexestrol dimethyl ether → erythro-3-aminohexestrol 4,4'-dimethyl ether (74536-56-4)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 36h; under 760 Torr; Ambient temperature;

DOI:10.1021/jm00183a007

Reference yield:

acetic acid-{5-[(1RS,2SR)-1-ethyl-2-(4-methoxy-phenyl)-butyl]-2-methoxy-anilide} → erythro-3-aminohexestrol 4,4'-dimethyl ether (74536-56-4)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01165a044

Reference yield:

1-{5-[(1RS,2SR)-1-ethyl-2-(4-methoxy-phenyl)-butyl]-2-methoxy-phenyl}-ethanone oxime → erythro-3-aminohexestrol 4,4'-dimethyl ether (74536-56-4)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₅; diethyl ether

2: methanol. NaOH

With sodium hydroxide; diethyl ether; phosphorus pentachloride;

DOI:10.1021/ja01165a044

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