[1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione

Base Information

Chemical Name:[1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione
CAS No.:1452228-36-2
Molecular Formula:C₁₅H₁₃F₃N₂O₄S
Molecular Weight:374.34
Hs Code.:

Synonyms:[1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione

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Chemical Property of [1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione

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Technology Process of [1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione

There total 3 articles about [1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1452228-35-1
1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethan-1-ol

: 1005-56-7
phenylcarbonochloridothioate

: 1452228-36-2
[1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 60186-89-2
4-bromo-2,6-dimethoxy-pyrimidine

: 1452228-36-2
[1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane; diethyl ether / 0.07 h / -78 °C

1.2: -78 - 20 °C

1.3: 20 °C

2.1: sodium tetrahydroborate / methanol / 2 h / 20 °C / Cooling with ice

3.1: dmap / dichloromethane / 2 h / 0 - 20 °C

With dmap; sodium tetrahydroborate; n-butyllithium; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane;

Reference yield:

: 1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethane-1,1-diol

: 1452228-36-2
[1-(2,6-dimethoxypyrimidin-4-yl)-2,2,2-trifluoroethoxy](phenoxy) methanethione

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 2 h / 20 °C / Cooling with ice

2: dmap / dichloromethane / 2 h / 0 - 20 °C

With dmap; sodium tetrahydroborate; In methanol; dichloromethane;