1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene

Base Information

• Chemical Name: 1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene
• CAS No.: 1300740-05-9
• Molecular Formula: C₉₃H₉₀N₁₂
• Molecular Weight: 1375.82
• Mol file: 1300740-05-9.mol

Synonyms:1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene

Chemical Property of 1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene

There total 1 articles about 1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,4,7,10,13,16-hexa-(pyrrole-2'-yl)-5,6,11,12,17,18-hexaazatrinaphtylene (1300740-02-6) + 4-octylbenzaldehyde (49763-66-8) → 1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene (1300740-05-9)

Guidance literature:

With trifluorormethanesulfonic acid; In dichloromethane; for 2h; Inert atmosphere; Microwave radiation;

Reference yield:

1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene (1300740-05-9) → 3C2H4O2*C93H81Fe3N12(9+)

Guidance literature:

With iron(II) acetate; In N,N-dimethyl-formamide; at 200 ℃; for 4h; Microwave irradiation;

Reference yield:

1,4,7,10,13,16-tris[2',2''-(4'''-octylphenylmethylene)bis-1H-pyrrole-5',5''-yl]-5,6,11,12,17,18-hexaazatrinaphthalene (1300740-05-9) + cobalt(II) diacetate tetrahydrate (6147-53-1) → 3C2H4O2*C93H83Co3N12

Guidance literature:

In N,N-dimethyl-formamide; at 200 ℃; for 2h; Microwave irradiation;

upstream raw materials:

1,4,7,10,13,16-hexa-(pyrrole-2'-yl)-5,6,11,12,17,18-hexaazatrinaphtylene

4-octylbenzaldehyde