C₂₉H₃₆O₇

Base Information

Chemical Name:C₂₉H₃₆O₇
CAS No.:1262406-17-6
Molecular Formula:C₂₉H₃₆O₇
Molecular Weight:496.601
Hs Code.:

C<sub>29</sub>H<sub>36</sub>O<sub>7</sub>

Synonyms:C₂₉H₃₆O₇

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Chemical Property of C₂₉H₃₆O₇

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Technology Process of C₂₉H₃₆O₇

There total 19 articles about C₂₉H₃₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1262324-72-0
15-O-acetyl-3-O-benzoylcharaciol

: 1262406-17-6
C₂₉H₃₆O₇

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/jo1019738

Reference yield:

: C₁₆H₃₀O₄Si

: 1262406-17-6
C₂₉H₃₆O₇

Guidance literature:: Multi-step reaction with 19 steps

1.1: decane / 180 °C

2.1: decane / 180 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 - 20 °C / Inert atmosphere

3.2: 0 °C

4.1: pyridinium p-toluenesulfonate

5.1: ozone; triphenylphosphine

6.1: triphenylphosphine

7.1: methyllithium

8.1: Schwartz's reagent; iodine

9.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 40 °C

9.2: 80 °C

10.1: lanthanum(III) nitrate hexahydrate / acetonitrile / 50 °C

11.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide

12.1: tetrahydrofuran / -78 °C / Inert atmosphere

13.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / pH 7

14.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide

15.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 2 h / 110 °C

16.1: pyridine; hydrogen fluoride

17.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2.5 h / 0 °C

18.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.17 h / 20 °C

19.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium aluminium tetrahydride; Schwartz's reagent; lanthanum(III) nitrate hexahydrate; trimethylsilyl trifluoromethanesulfonate; hydrogen fluoride; methyllithium; iodine; pyridinium p-toluenesulfonate; ozone; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; decane; dichloromethane; water; dimethyl sulfoxide; toluene; acetonitrile; 9.2: Suzuki-Miyaura cross-coupling / 17.1: Mitsunobu reaction;
DOI:10.1021/jo1019738

Reference yield:

: 1114553-44-4
C₁₅H₃₀O₃Si

: 1262406-17-6
C₂₉H₃₆O₇

Guidance literature:: Multi-step reaction with 16 steps

1.1: pyridinium p-toluenesulfonate

2.1: ozone; triphenylphosphine

3.1: triphenylphosphine

4.1: methyllithium

5.1: Schwartz's reagent; iodine

6.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 40 °C

6.2: 80 °C

7.1: lanthanum(III) nitrate hexahydrate / acetonitrile / 50 °C

8.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide

9.1: tetrahydrofuran / -78 °C / Inert atmosphere

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / pH 7

11.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide

12.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 2 h / 110 °C

13.1: pyridine; hydrogen fluoride

14.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 2.5 h / 0 °C

15.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.17 h / 20 °C

16.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; Schwartz's reagent; lanthanum(III) nitrate hexahydrate; trimethylsilyl trifluoromethanesulfonate; hydrogen fluoride; methyllithium; iodine; pyridinium p-toluenesulfonate; ozone; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene; acetonitrile; 6.2: Suzuki-Miyaura cross-coupling / 14.1: Mitsunobu reaction;
DOI:10.1021/jo1019738