2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide

Base Information

• Chemical Name: 2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide
• CAS No.: 1150698-06-8
• Molecular Formula: C₂₅H₃₅BN₂O₃
• Molecular Weight: 422.375

Synonyms:2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide

Chemical Property of 2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide

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Technology Process of 2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide

There total 1 articles about 2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C30H43BN2O5 (1150697-36-1) → 2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide (1150698-06-8)

Guidance literature:

With hydrogenchloride; In chloroform; ethyl acetate; at 20 ℃; for 2h;

DOI:10.1021/jm900125m

Reference yield: 64.0%

2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide (1150698-06-8) + benzoic acid (65-85-0,8013-63-6) → 1-(biphenyl-3-ylaminocarbonyl)-6-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)hexylbenzamide (1150697-70-3)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1021/jm900125m

Reference yield: 41.0%

2-amino-N-(biphenyl-3-yl)-7-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)heptanamide (1150698-06-8) + benzyl chloroformate (501-53-1,94274-21-2) → benzyl 1-(biphenyl-3-ylaminocarbonyl)-6-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)hexylcarbamate (1150697-68-9)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jm900125m

upstream raw materials:

C₃₀H₄₃BN₂O₅

Downstream raw materials:

C₃₁H₃₈BN₃O₄

C₂₉H₃₆BN₃O₄S

C₂₉H₃₆BN₃O₄S

C₃₄H₄₀BN₃O₄

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