5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide

Base Information

Chemical Name:5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide
CAS No.:1079991-20-0
Molecular Formula:C₂₂H₂₈BrNO₄Si
Molecular Weight:478.458
Hs Code.:

Synonyms:5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide

Suppliers and Price of 5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide

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Technology Process of 5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide

There total 1 articles about 5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 173901-21-8
4-(2-{[tert-butyl(dimethyl)silyl]oxy}ethyl)aniline

: 957765-79-6
6-bromo-2,3-(methylenedioxy)benzoyl chloride

: 1079991-20-0
5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jm8005433

Reference yield: 80.0%

: 13057-17-5
bromethyl methyl ether

: 1079991-20-0
5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide

: 1079991-23-3
5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)-N-(methoxymerthyl)benzo[d][1,3]dioxole-4-carboxamide

Guidance literature:: 5-bromo-N-(4-(tert-butyldimethylsilyloxyethyl)phenyl)benzo[d][1,3]dioxole-4-carboxamide; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.333333h; Inert atmosphere;

bromethyl methyl ether; In tetrahydrofuran; mineral oil; at 40 ℃; for 3h;
DOI:10.1021/jm8005433