Technology Process of C68H45BrN2
There total 3 articles about C68H45BrN2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1007/s10895-010-0732-z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide / tetrahydrofuran; water; dimethyl sulfoxide / 4 h / 80 °C
1.2: 20 °C
2.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 20 °C
2.2: 6 h / 70 °C
3.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
With
potassium tert-butylate; potassium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
3.1: Wittig-Horner reaction;
DOI:10.1007/s10895-010-0732-z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Aliquat 336; potassium carbonate / water; toluene / 0.75 h / 20 °C / Inert atmosphere
1.2: 16 h / 85 °C / Inert atmosphere
2.1: potassium hydroxide / tetrahydrofuran; water; dimethyl sulfoxide / 4 h / 80 °C
2.2: 20 °C
3.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 20 °C
3.2: 6 h / 70 °C
4.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
With
potassium tert-butylate; Aliquat 336; potassium carbonate; potassium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
1.1: Suzuki coupling / 1.2: Suzuki coupling / 4.1: Wittig-Horner reaction;
DOI:10.1007/s10895-010-0732-z
