2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline

Base Information

Chemical Name:2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline
CAS No.:1375798-11-0
Molecular Formula:C₂₁H₁₇N₃S
Molecular Weight:343.452
Hs Code.:

Synonyms:2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline

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Chemical Property of 2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline

Chemical Property:

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Technology Process of 2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline

There total 7 articles about 2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84570-86-5
6-chloro-2-(6-methylpyridin-2-yl)-4-phenylquinazoline

: 5188-07-8
sodium thiomethoxide

: 1375798-11-0
2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline

Guidance literature:: In methanol; at 150 ℃; for 1h; microwave irradiation;

Reference yield:

: 109-06-8
α-picoline

: 1375798-11-0
2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline

Guidance literature:: Multi-step reaction with 7 steps

1.1: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 0 - 20 °C

2.1: carbamic chloride / toluene / 0.67 h / 70 °C / microwave irradiation

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

3.2: Reflux

3.3: 0 °C

4.1: hydrogenchloride; water / 6 h / 150 °C / pressure vessel

5.1: phosphorus(V) oxybromide / 0 - 110 °C

6.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane / Inert atmosphere; Reflux

7.1: methanol / 1 h / 150 °C / microwave irradiation

With hydrogenchloride; carbamic chloride; water; sodium hydride; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; phosphorus(V) oxybromide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethyl acetate; toluene; mineral oil;

Reference yield:

: 1620-75-3
2-Cyano-6-methylpyridine

: 1375798-11-0
2-(6-methyl-2-pyridyl)-6-methylsulfanyl-4-phenylquinazoline

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

1.2: Reflux

1.3: 0 °C

2.1: hydrogenchloride; water / 6 h / 150 °C / pressure vessel

3.1: phosphorus(V) oxybromide / 0 - 110 °C

4.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane / Inert atmosphere; Reflux

5.1: methanol / 1 h / 150 °C / microwave irradiation

With hydrogenchloride; water; sodium hydride; sodium carbonate; phosphorus(V) oxybromide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; mineral oil;