(Dimethylphenylsilyl)acetylene

Base Information

Chemical Name:(Dimethylphenylsilyl)acetylene
CAS No.:17156-64-8
Molecular Formula:C10H12 Si
Molecular Weight:160.291
Hs Code.:2931900090
DSSTox Substance ID:DTXSID90399112
Nikkaji Number:J316.653H
Wikidata:Q82201476
Mol file:17156-64-8.mol

Synonyms:(Dimethylphenylsilyl)acetylene;17156-64-8;ethynyl-dimethyl-phenylsilane;(DIMETHYLPHENYLSILYL)ACETYLENE 98;Ethynylphenyldimethylsilane;dimethylphenylsilylacetylene;ETHYNYLDIMETHYLPHENYLSILANE;DTXSID90399112;(Dimethylphenylsilyl)acetylene, 98%;AKOS015913592;J-010734

Suppliers and Price of (Dimethylphenylsilyl)acetylene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
(Dimethylphenylsilyl)acetylene 98%
5g
$ 400.00

Sigma-Aldrich
(Dimethylphenylsilyl)acetylene 98%
1g
$ 118.00

American Custom Chemicals Corporation
(DIMETHYLPHENYLSILYL)ACETYLENE 95.00%
5G
$ 1130.28

American Custom Chemicals Corporation
(DIMETHYLPHENYLSILYL)ACETYLENE 95.00%
1G
$ 705.45

Total 3 raw suppliers

Chemical Property of (Dimethylphenylsilyl)acetylene

Chemical Property:

Vapor Pressure:1.21mmHg at 25°C
Melting Point:158-164 °C(Solv: chloroform (67-66-3); hexane (110-54-3))
Refractive Index:n20/D 1.508(lit.)
Boiling Point:34 °C0.07 mm Hg(lit.)
Flash Point:135 °F
PSA：0.00000
Density:0.907 g/mL at 25 °C(lit.)
LogP:1.77440
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:160.070826917
Heavy Atom Count:11
Complexity:167

Purity/Quality:

98%Min ^*data from raw suppliers

(Dimethylphenylsilyl)acetylene 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C#C)C1=CC=CC=C1

Technology Process of (Dimethylphenylsilyl)acetylene

There total 6 articles about (Dimethylphenylsilyl)acetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 768-33-2
phenyldimethylsilyl chloride

: 4301-14-8
acetylenemagnesium bromide

: 17156-64-8
(dimethylphenylsilyl)acetylene

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jo070039n

Reference yield: 86.0%

: 768-33-2
phenyldimethylsilyl chloride

: 74-86-2,25067-58-7
acetylene

: 17156-64-8
(dimethylphenylsilyl)acetylene

Guidance literature:: With ethylmagnesium bromide; In tetrahydrofuran; for 36h; Heating;
DOI:10.1016/S0040-4020(01)90571-X

Reference yield: 52.0%

: 1066-26-8
sodium acetylide

: 768-33-2
phenyldimethylsilyl chloride

: 17156-64-8
(dimethylphenylsilyl)acetylene

Guidance literature:: In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; mineral oil; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201402145