phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside
CAS No.:173207-92-6
Molecular Formula:C₆₇H₅₄O₁₇S
Molecular Weight:1163.22
Hs Code.:

Synonyms:phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside

There total 3 articles about phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 14218-11-2,14218-30-5,61198-88-7,108438-33-1,108836-02-8,114682-36-9,127305-34-4,151377-77-4
2,3,4,6-Tetra-O-benzoyl-α-D-mannopyranosyl bromide

: 150935-65-2
phenyl 2,3,4-tri-O-benzoyl-1-thio-α-D-mannopyranoside

: 173207-92-6
phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With 3 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at -45 - -40 ℃; for 2h;

Reference yield:

: 150935-64-1
phenyl 2,3,4-tri-O-benzoyl-6-O-tert-butyldimethylsilyl-1-thio-α-D-mannopyranoside

: 173207-92-6
phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / acetic acid / tetrahydrofuran; H₂O / 168 h

2: 86 percent / molecular sieves (3 Angstroem), silver triflate / CH₂Cl₂ / 2 h / -45 - -40 °C

With 3 A molecular sieve; silver trifluoromethanesulfonate; acetic acid; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 2592-58-7,3006-48-2,3006-49-3,13526-09-5,14679-57-3,22415-91-4,29884-70-6,41545-55-5,41545-56-6,41569-33-9,96996-90-6,121570-85-2,121570-86-3
1,2,3,4,6-penta-O-benzoyl-α-D-mannopyranoside

: 173207-92-6
phenyl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / HBr, molecular sieves (3 Angstroem) / CH₂Cl₂; acetic acid / 4 °C

2: 86 percent / molecular sieves (3 Angstroem), silver triflate / CH₂Cl₂ / 2 h / -45 - -40 °C

With 3 A molecular sieve; hydrogen bromide; silver trifluoromethanesulfonate; In dichloromethane; acetic acid;