Pd⁽²⁺⁾*C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2^(1-)*CF₃COO^(1-)=[Pd(C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2)(CF₃COO)]

Base Information

• Chemical Name: Pd⁽²⁺⁾*C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2^(1-)*CF₃COO^(1-)=[Pd(C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2)(CF₃COO)]
• CAS No.: 251912-34-2
• Molecular Formula: C₂F₃O₂*C₂₇H₂₃OS₂*Pd
• Molecular Weight: 647.047

Synonyms:Pd⁽²⁺⁾*C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2^(1-)*CF₃COO^(1-)=[Pd(C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2)(CF₃COO)]

Chemical Property of Pd⁽²⁺⁾*C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2^(1-)*CF₃COO^(1-)=[Pd(C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2)(CF₃COO)]

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Technology Process of Pd⁽²⁺⁾*C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2^(1-)*CF₃COO^(1-)=[Pd(C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2)(CF₃COO)]

There total 1 articles about Pd⁽²⁺⁾*C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2^(1-)*CF₃COO^(1-)=[Pd(C₆H₅CH₂OC₆H₂(CH₂SC₆H₅)2)(CF₃COO)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

palladium(II) trifluoroacetate + O-benzyl-3,5-bis(phenylthiomethyl)phenol (251912-33-1) → Pd(2+)*C6H5CH2OC6H2(CH2SC6H5)2(1-)*CF3COO(1-)=[Pd(C6H5CH2OC6H2(CH2SC6H5)2)(CF3COO)] (251912-34-2)

Guidance literature:

In N,N-dimethyl-formamide; N2 atmosphere, stirring (2.5 h, room temp.); pouring into diethyl ether (pptn.), cooling (-5°C, 16 h), removalof supernatant, washing (ether), drying (vac.);

DOI:10.1021/ja991099g

upstream raw materials:

O-benzyl-3,5-bis(phenylthiomethyl)phenol

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