7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one

Base Information

Chemical Name:7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one
CAS No.:932749-51-4
Molecular Formula:C₂₆H₂₂N₂O₂S
Molecular Weight:426.539
Hs Code.:

Synonyms:7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one

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Chemical Property of 7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one

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Technology Process of 7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one

There total 4 articles about 7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 932749-43-4
8-(2,4-dimethyl-phenoxymethyl)-10-phenyl-6,10-dihydro-5-thia-1,10-diaza-phenanthren-9-one

: 932749-51-4
7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one

Guidance literature:: With aluminium trichloride; In dichloromethane; at 20 ℃;
DOI:10.1139/V06-174

Reference yield:

: 932749-27-4
4-mercapto-1-phenyl-1,8-naphthyridin-2(1H)-one

: 932749-51-4
7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / benzyltriethylammonium chloride; NaOH / H₂O / 20 °C

2: 85 percent / chlorobenzene / 132 °C

3: 75 percent / anhydrous AlCl₃ / CH₂Cl₂ / 20 °C

With sodium hydroxide; aluminium trichloride; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water; chlorobenzene; 3: Claisen rearrangement;
DOI:10.1139/V06-174

Reference yield:

: 932749-35-4
4-[4-(2,4-dimethyl-phenoxy)-but-2-ynylsulfanyl]-1-phenyl-1H-[1,8]naphthyridin-2-one

: 932749-51-4
7-(2-hydroxy-3,5-dimethyl-phenyl)-8-methylene-10-phenyl-6,7,8,10-tetrahydro-5-thia-1,10-diaza-phenanthren-9-one

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / chlorobenzene / 132 °C

2: 75 percent / anhydrous AlCl₃ / CH₂Cl₂ / 20 °C

With aluminium trichloride; In dichloromethane; chlorobenzene; 2: Claisen rearrangement;
DOI:10.1139/V06-174