5-amino-2-methylaminobenzoic acid hydrazide

Base Information

Chemical Name:5-amino-2-methylaminobenzoic acid hydrazide
CAS No.:77423-09-7
Molecular Formula:C₈H₁₂N₄O
Molecular Weight:180.209
Hs Code.:

Synonyms:5-amino-2-methylaminobenzoic acid hydrazide

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Chemical Property of 5-amino-2-methylaminobenzoic acid hydrazide

Chemical Property:

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Technology Process of 5-amino-2-methylaminobenzoic acid hydrazide

There total 2 articles about 5-amino-2-methylaminobenzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 77423-11-1
2-Methylamino-5-nitro-benzoic acid hydrazide

: 77423-09-7
5-amino-2-methylaminobenzoic acid hydrazide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 46h;
DOI:10.1021/jm00138a019

Reference yield:

: 4693-01-0
1-methyl-6-nitro-2H-benzo-[d][1,3]oxazine-2,4(1H)-dione

: 77423-09-7
5-amino-2-methylaminobenzoic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 18percent aq. NH₂NH₂ / Ambient temperature

2: 85 percent / H₂ / 5percent Pd/C / methanol; tetrahydrofuran / 46 h

With hydrogen; hydrazine hydrate; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm00138a019

Reference yield:

: 77423-09-7
5-amino-2-methylaminobenzoic acid hydrazide

: 77422-99-2
PD 90780

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) Na₂CO₃ / 1.) water, reflux, 1.5 h, 2.) water, reflux, 1 h

2: 18 percent / 22 h / Heating

With sodium carbonate;
DOI:10.1021/jm00138a019