1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide

Base Information

Chemical Name:1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide
CAS No.:82691-78-9
Molecular Formula:C₉H₁₃F₃N₂O₂
Molecular Weight:238.21
Hs Code.:

Synonyms:1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide

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Chemical Property of 1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide

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Technology Process of 1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide

There total 3 articles about 1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 82691-76-7
N-<(2,2,2-trifluoroethylidene)amino>-1-cyclohexenecarboximidoyl chloride

: 82691-78-9
1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide

: 82691-77-8
1-cyclohexenecarboxylic acid 2-(2,2,2-trifluoroethylidene)hydrazide

Guidance literature:: With water; In tetrahydrofuran; at 50 ℃; for 0.166667h;
DOI:10.1021/jo00141a012

Reference yield:

: 80967-56-2,80967-61-9
4-chloro-2-(1-chloro-2,2,2-trifluoroethyl)-1-thia-2,3-diazaspiro<4.5>dec-3-ene 1-oxide

: 82691-78-9
1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / 85percent m-chloroperbenzoic acid / CHCl₃ / 1.) a) 65-70 deg C, 1 h, b) RT, overnight

2: 71 percent / toluene / 2 h / Heating

3: 3 percent / H₂O / tetrahydrofuran / 0.17 h / 50 °C

With water; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; chloroform; toluene;
DOI:10.1021/jo00141a012

Reference yield:

: 80967-59-5
4-chloro-2-(1-chloro-2,2,2-trifluoroethyl)-1-thia-2,3-diazaspiro<4.5>dec-3-ene 1,1-dioxide

: 82691-78-9
1-cyclohexenecarboxylic acid 2-(1-hydroxy-2,2,2-trifluoroethyl)hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / toluene / 2 h / Heating

2: 3 percent / H₂O / tetrahydrofuran / 0.17 h / 50 °C

With water; In tetrahydrofuran; toluene;
DOI:10.1021/jo00141a012