2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone

Base Information

Chemical Name:2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone
CAS No.:103789-39-5
Molecular Formula:C₂₃H₂₃N₃O₃S₂
Molecular Weight:453.586
Hs Code.:

Synonyms:2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone

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Chemical Property of 2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone

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Technology Process of 2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone

There total 6 articles about 2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[5-Methyl-2-(3-methylsulfanyl-phenyl)-oxazol-4-yl]-ethanol

: 103789-39-5
2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / dimethylformamide / 1 h / Ambient temperature

2: H₂ / 10 percent Pd/C / methanol / Ambient temperature

3: 1.) aq. NaNO₂, aq. HBr, 2.) Cu₂O / 1.) MeOH, acetone, 5 deg C, 30 min, 2.) MeOH, acetone, 38 deg C

4: NaOAc / ethanol / 3 h / Heating

With copper(I) oxide; hydrogen bromide; hydrogen; sodium acetate; sodium hydride; sodium nitrite; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00092a012

Reference yield:

: 103789-25-9
4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}nitrobenzene

: 103789-39-5
2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10 percent Pd/C / methanol / Ambient temperature

2: 1.) aq. NaNO₂, aq. HBr, 2.) Cu₂O / 1.) MeOH, acetone, 5 deg C, 30 min, 2.) MeOH, acetone, 38 deg C

3: NaOAc / ethanol / 3 h / Heating

With copper(I) oxide; hydrogen bromide; hydrogen; sodium acetate; sodium nitrite; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00092a012

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 103789-39-5
2-imino-5-<4-{2-[5-methyl-2-(3-methylthiophenyl)-4-oxazolyl]ethoxy}benzyl>-4-thiazolidinone

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / dimethylformamide / 1 h / Ambient temperature

2: H₂ / 10 percent Pd/C / methanol / Ambient temperature

3: 1.) aq. NaNO₂, aq. HBr, 2.) Cu₂O / 1.) MeOH, acetone, 5 deg C, 30 min, 2.) MeOH, acetone, 38 deg C

4: NaOAc / ethanol / 3 h / Heating

With copper(I) oxide; hydrogen bromide; hydrogen; sodium acetate; sodium hydride; sodium nitrite; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00092a012