N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine]

Base Information

Chemical Name:N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine]
CAS No.:247210-69-1
Molecular Formula:C₂₄H₃₈N₃O₇PS₂
Molecular Weight:575.687
Hs Code.:

Synonyms:N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine]

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Chemical Property of N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine]

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Technology Process of N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine]

There total 4 articles about N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 90974-12-2
N-diethoxyphosphoryl-3,3'-iminodipropionitrile

: 98-59-9
p-toluenesulfonyl chloride

: 247210-69-1
N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine]

Guidance literature:: N-diethoxyphosphoryl-3,3'-iminodipropionitrile; With ammonia; hydrogen; Raney nickel; In methanol; for 48h; under 2327.23 Torr;

p-toluenesulfonyl chloride; With triethylamine; In dichloromethane; at 20 ℃;

Reference yield: 43.0%

: 98-59-9
p-toluenesulfonyl chloride

: 247210-68-0
N-diethoxyphosphoryl-3,3'-iminobis[propylamine]

: 247210-69-1
N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine]

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jm990211i

Reference yield:

: 111-94-4
3,3'-Iminodipropionitrile

: 247210-69-1
N-diethoxyphosphoryl-N',N''-bis(p-toluenesulfonyl)-3,3'-iminobis[propylamine]

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / Et₃N / CH₂Cl₂ / 20 °C

2: 92 percent / H₂, NH₃ / Raney nickel / methanol / 48 h / 20 °C / 2327.17 Torr

3: 43 percent / Et₃N / CH₂Cl₂ / 20 °C

With ammonia; hydrogen; triethylamine; nickel; In methanol; dichloromethane; 1: protection of the amino group / 2: Hydrogenation / 3: Tosylation;
DOI:10.1021/jm990211i