(2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

Base Information

Chemical Name:(2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one
CAS No.:1202071-77-9
Molecular Formula:C₂₀H₂₀O₆
Molecular Weight:356.375
Hs Code.:

Synonyms:(2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

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Chemical Property of (2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

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Technology Process of (2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

There total 1 articles about (2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 2879-20-1
1,4-benzodioxan-6-yl methyl ketone

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1202071-77-9
(2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

Guidance literature:: With sodium hydroxide; In methanol; water; at 20 ℃;
DOI:10.1016/j.bmc.2009.09.039

Reference yield:

: 1202071-77-9
(2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

: (2,3-dihydro-1,4-benzodioxin-6-yl)[3-(3,4,5-trimethoxyphenyl)oxiran-2-yl]methanone

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In ethanol; at 20 - 30 ℃; for 57h;
DOI:10.1021/acscombsci.8b00113

Reference yield:

: 1202071-77-9
(2E)-1-(2,3-dihydro-1,4-benzodioxin-6-yl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

: 3-(2,3-d-dihydro-1,4-benzodioxin-6-yl)-3-oxo-2-(3,4,5-trimethoxyphenyl)propanal

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; sodium hydroxide / ethanol / 57 h / 20 - 30 °C

2: boron trifluoride diethyl etherate / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; dihydrogen peroxide; sodium hydroxide; In ethanol; dichloromethane;
DOI:10.1021/acscombsci.8b00113