C₃₉H₅₀N₂O₁₁Si

Base Information

Chemical Name:C₃₉H₅₀N₂O₁₁Si
CAS No.:1280608-67-4
Molecular Formula:C₃₉H₅₀N₂O₁₁Si
Molecular Weight:750.918
Hs Code.:

C<sub>39</sub>H<sub>50</sub>N<sub>2</sub>O<sub>11</sub>Si

Synonyms:C₃₉H₅₀N₂O₁₁Si

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Chemical Property of C₃₉H₅₀N₂O₁₁Si

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Technology Process of C₃₉H₅₀N₂O₁₁Si

There total 10 articles about C₃₉H₅₀N₂O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 19788-36-4
4-hydroxymethyl-3,5-dimethylisoxazole

: 1280608-62-9
C₃₃H₄₁NO₉Si

: 1280608-67-4
C₃₉H₅₀N₂O₁₁Si

Guidance literature:: 4-hydroxymethyl-3,5-dimethylisoxazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

C₃₃H₄₁NO₉Si; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-51-6
C₃₀H₃₃NO₆

: 1280608-67-4
C₃₉H₅₀N₂O₁₁Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

2.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

3.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

4.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

6.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

7.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

7.2: -78 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; Oxone; n-butyllithium; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; Dimethoxymethane; hexane; dichloromethane; water; acetonitrile; 1.1: Shi epoxidation / 6.1: Dess-Martin oxidation;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-40-3
C₂₃H₂₅NO₆

: 1280608-67-4
C₃₉H₅₀N₂O₁₁Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 2.5 h / 20 °C

3.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

4.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

5.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

6.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

7.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

9.2: -78 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; Oxone; sodium tetrahydroborate; n-butyllithium; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; Dimethoxymethane; hexane; dichloromethane; water; acetonitrile; mineral oil; 3.1: Shi epoxidation / 8.1: Dess-Martin oxidation;
DOI:10.1002/anie.201006528