Technology Process of methyl 14-oxo-16-(triphenylmethoxy)isopimarate
There total 4 articles about methyl 14-oxo-16-(triphenylmethoxy)isopimarate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
for 1h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) sodium boranuide, BF3, 2.) aq. NaOH, 30percent H2O2 / 1.) diglyme, room temperature, 3 h, 2.) 0 deg C, 1 h; room temperature, overnight
2: 78 percent / Et3N, 4-dimethylpyridine / dimethylformamide / 7 h / Ambient temperature
3: 82 percent / CrO3 / pyridine; CH2Cl2 / 0.5 h
4: 100 percent / NaOMe / methanol / 1 h / Heating
With
chromium(VI) oxide; sodium hydroxide; sodium tetrahydroborate; 4-dimethylpyridine; boron trifluoride; dihydrogen peroxide; sodium methylate; triethylamine;
In
pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 78 percent / Et3N, 4-dimethylpyridine / dimethylformamide / 7 h / Ambient temperature
2: 82 percent / CrO3 / pyridine; CH2Cl2 / 0.5 h
3: 100 percent / NaOMe / methanol / 1 h / Heating
With
chromium(VI) oxide; 4-dimethylpyridine; sodium methylate; triethylamine;
In
pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;
