C₂₂H₃₂F₃NO₆S*ClH

Base Information

Chemical Name:C₂₂H₃₂F₃NO₆S*ClH
CAS No.:1413281-99-8
Molecular Formula:C₂₂H₃₂F₃NO₆S*ClH
Molecular Weight:532.021
Hs Code.:

C<sub>22</sub>H<sub>32</sub>F<sub>3</sub>NO<sub>6</sub>S*ClH

Synonyms:C₂₂H₃₂F₃NO₆S*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₂F₃NO₆S*ClH

Chemical Property:

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Technology Process of C₂₂H₃₂F₃NO₆S*ClH

There total 4 articles about C₂₂H₃₂F₃NO₆S*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1413281-98-7
C₂₂H₃₀F₃NO₈S

: 1413281-99-8
C₂₂H₃₂F₃NO₆S*ClH

Guidance literature:: C₂₂H₃₀F₃NO₈S; With sodium tetrahydroborate; zirconium(IV) chloride; In tetrahydrofuran; at 0 - 20 ℃; for 4h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield:

: 1310055-50-5
C₁₄H₂₃NO₆

: 1413281-99-8
C₂₂H₃₂F₃NO₆S*ClH

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / acetonitrile / 4.5 h / 0 - 40 °C / Inert atmosphere

2.1: aluminum (III) chloride / dichloromethane / 1.75 h / 30 - 40 °C / Inert atmosphere

2.2: Cooling with ice

3.1: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / dichloromethane / 0 - 5 °C / Inert atmosphere

4.1: zirconium(IV) chloride; sodium tetrahydroborate / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

With aluminum (III) chloride; sodium tetrahydroborate; oxalyl dichloride; 1,1,3,3-Tetramethyldisiloxane; zirconium(IV) chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; acetonitrile; 2.1: Friedel Crafts Acylation;

Reference yield:

: 1310055-51-6
C₁₄H₂₂ClNO₅

: 1413281-99-8
C₂₂H₃₂F₃NO₆S*ClH

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / dichloromethane / 1.75 h / 30 - 40 °C / Inert atmosphere

1.2: Cooling with ice

2.1: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / dichloromethane / 0 - 5 °C / Inert atmosphere

3.1: zirconium(IV) chloride; sodium tetrahydroborate / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

With aluminum (III) chloride; sodium tetrahydroborate; 1,1,3,3-Tetramethyldisiloxane; zirconium(IV) chloride; In tetrahydrofuran; dichloromethane; 1.1: Friedel Crafts Acylation;