1-(4-toluidino)ethylferrocene

Base Information

Chemical Name:1-(4-toluidino)ethylferrocene
CAS No.:727651-97-0
Molecular Formula:C₁₉H₂₁FeN
Molecular Weight:319.229
Hs Code.:

Synonyms:1-(4-toluidino)ethylferrocene

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Chemical Property of 1-(4-toluidino)ethylferrocene

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Technology Process of 1-(4-toluidino)ethylferrocene

There total 3 articles about 1-(4-toluidino)ethylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: (S)-(-)-(1-trimethylammonio)ethylferrocene iodide

: 106-49-0,12221-03-3
p-toluidine

: 727651-97-0
1-(4-toluidino)ethylferrocene

Guidance literature:: With potassium carbonate; In solid; mixt. methoiodide, amine, and K2CO3 was heated for 2 h in oil bath at 70°C; react. mixt. was extd. with chloroform and filtered, residue was chromed. on silica (CHCl3-MeOH); elem. anal.;
DOI:10.1023/B:RUCB.0000011870.91892.43

Reference yield: 66.0%

: 155890-37-2,176911-04-9,160262-71-5
[(η(5)-C5H5)Fe(η(5)-C5H4-C(CH3)=N-C6H4-4-CH3)]

: 727651-97-0
1-(4-toluidino)ethylferrocene

Guidance literature:: [(η(5)-C5H5)Fe(η(5)-C5H4-C(CH3)=N-C6H4-4-CH3)]; With chloro(η⁵-cyclopentadienyl)(1,3-dimesitylimidazol-2-ylidene)nickel(II); NaH*C₆H₁₅B; diphenylsilane; In tetrahydrofuran; at 70 ℃; for 17h;

With methanol; sodium hydroxide; In tetrahydrofuran; at 25 ℃; for 2h; Temperature; Concentration;
DOI:10.1039/c3cy00514c

Reference yield: 57.0%

: 155890-37-2,176911-04-9,160262-71-5
[(η(5)-C5H5)Fe(η(5)-C5H4-C(CH3)=N-C6H4-4-CH3)]

: 694-53-1
phenylsilane

: 727651-97-0
1-(4-toluidino)ethylferrocene

Guidance literature:: With NaOH; [CpFe(IMes)(CO₂)]I; In toluene; Irradiation (UV/VIS); aldimine (0.5 mmol), PhSiH3 (1 mmol) and Fe complex (5 mol %) in tolueneirradiated with visible light (stirring, 100°C, 24 h); hydrolyze d with 2 M aq. NaOH and MeOH;
DOI:10.1039/c1cc14403k