Technology Process of C20H22O2Se
There total 3 articles about C20H22O2Se which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere
2: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere
With
sodium benzoate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / methanol / 3 h / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere
3: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere
With
sodium benzoate; sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid;
In
methanol; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
2: sodium tetrahydroborate / methanol / 3 h / Inert atmosphere
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere
4: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere
With
sodium benzoate; sodium tetrahydroborate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114