2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside

Base Information

Chemical Name:2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside
CAS No.:1304042-90-7
Molecular Formula:C₅₂H₇₁N₄O₁₆S₂*Na
Molecular Weight:1095.27
Hs Code.:

2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside

Synonyms:2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside

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Chemical Property of 2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside

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Technology Process of 2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside

There total 16 articles about 2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 773837-37-9
sodium cyanide

: 1304042-87-2
2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4,6-cyclic sulfate-α-D-mannopyranoside

: 1304042-90-7
2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

: 4163-65-9
per-O-acetyl-α-D-mannopyranose

: 1304042-90-7
2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 8 h / 20 °C

2.1: sodium azide / N,N-dimethyl-formamide / 4 h / 65 °C

3.1: sodium methylate / methanol / 0.5 h / 20 °C

3.2: amberlyst IRC-50-H+ resin beads

4.1: toluene-4-sulfonic acid / acetone / 4 h / 20 °C

5.1: thionyl chloride; triethylamine / dichloromethane / 0.08 h / 0 °C / Cooling with ice

6.1: sodium periodate / ruthenium trichloride / dichloromethane; acetonitrile; water / 1 h / 20 °C

7.1: copper(ll) sulfate pentahydrate; L-ascorbic acid sodium salt / dichloromethane; water / 24 h / 20 °C

8.1: N,N-dimethyl-formamide / 4 h / 20 °C

With sodium periodate; thionyl chloride; sodium azide; copper(ll) sulfate pentahydrate; L-ascorbic acid sodium salt; boron trifluoride diethyl etherate; sodium methylate; triethylamine; ruthenium trichloride; toluene-4-sulfonic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 140428-83-7
2-azidoethyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

: 1304042-90-7
2-{4-[27-(4-methoxyphenyl)-27,27-diphenyl-2,5,8,11,14,17,20-heptaoxa-26-thiaheptacos-1-yl]-2,3-dihydro-1H-1,2,3,-triazol-1-yl}ethyl-6-deoxy-2,3-O-(1-methylethylidene)-4-sodium sulfate-6-cyano-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium methylate / methanol / 0.5 h / 20 °C

1.2: amberlyst IRC-50-H+ resin beads

2.1: toluene-4-sulfonic acid / acetone / 4 h / 20 °C

3.1: thionyl chloride; triethylamine / dichloromethane / 0.08 h / 0 °C / Cooling with ice

4.1: sodium periodate / ruthenium trichloride / dichloromethane; acetonitrile; water / 1 h / 20 °C

5.1: copper(ll) sulfate pentahydrate; L-ascorbic acid sodium salt / dichloromethane; water / 24 h / 20 °C

6.1: N,N-dimethyl-formamide / 4 h / 20 °C

With sodium periodate; thionyl chloride; copper(ll) sulfate pentahydrate; L-ascorbic acid sodium salt; sodium methylate; triethylamine; ruthenium trichloride; toluene-4-sulfonic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;