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Technology Process of [(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)](1+)*PF6(1-)=[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)]PF6

[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)](1+)*PF6(1-)=[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)]PF6

Base Information
  • Chemical Name:[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)](1+)*PF6(1-)=[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)]PF6
  • CAS No.:99898-15-4
  • Molecular Formula:C12H25CoIP2*F6P
  • Molecular Weight:562.14
  • Hs Code.:
[(C<sub>5</sub>H<sub>5</sub>)CoI(CH<sub>2</sub>P(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)]<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[(C<sub>5</sub>H<sub>5</sub>)CoI(CH<sub>2</sub>P(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)]PF<sub>6</sub>

Synonyms:[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)](1+)*PF6(1-)=[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)]PF6

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Chemical Property of [(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)](1+)*PF6(1-)=[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)]PF6
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Technology Process of [(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)](1+)*PF6(1-)=[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)]PF6

There total 1 articles about [(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)](1+)*PF6(1-)=[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

ammonium hexafluorophosphate

ammonium hexafluorophosphate

carbonyl(cyclopentadienyl)(trimethylphosphane)cobalt
66652-86-6

carbonyl(cyclopentadienyl)(trimethylphosphane)cobalt

diiodomethane
75-11-6

diiodomethane

dicarbonylcyclopentadienylcobalt
12078-25-0,12078-23-8

dicarbonylcyclopentadienylcobalt

[(C<sub>5</sub>H<sub>5</sub>)CoI(CH<sub>2</sub>P(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)]<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=[(C<sub>5</sub>H<sub>5</sub>)CoI(CH<sub>2</sub>P(CH<sub>3</sub>)3)(P(CH<sub>3</sub>)3)]PF<sub>6</sub>
99898-15-4

[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)](1+)*PF6(1-)=[(C5H5)CoI(CH2P(CH3)3)(P(CH3)3)]PF6

Guidance literature:
With (C2H5)3N; In methanol; toluene; under N2; to soln. of Co complex and NEt3 in C6H5CH3 dropwise added CH2I2 at 0 °C, added pentane, filtered, washed with pentane, dried in vac., NH4PF6 added, added MeOH, stirred for 10 min; added Et2O, filtered, recrystd. (acetone/Et2O); elem. anal.;
DOI:10.1016/0022-328X(85)88035-9
upstream raw materials:

carbonyl(cyclopentadienyl)(trimethylphosphane)cobalt

diiodomethane

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