Technology Process of C24H33F3O5Si
There total 3 articles about C24H33F3O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C24H31F3O5Si;
With
B-chlorodiisopinocampheylborane;
In
tetrahydrofuran; n-heptane;
at -30 - -25 ℃;
Inert atmosphere;
With
methanol; sodium hydrogencarbonate;
In
tetrahydrofuran; n-heptane;
at 20 ℃;
for 10h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere
1.2: 1.5 h / 0 °C
2.1: (-)-diisopinocamphenylborane chloride / n-heptane; tetrahydrofuran / 5 h / -30 - -25 °C / Inert atmosphere
2.2: 10 h / 20 °C
With
sodium hydride; (-)-diisopinocamphenylborane chloride;
In
tetrahydrofuran; n-heptane; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere
1.2: 1.5 h / 0 °C
2.1: (-)-diisopinocamphenylborane chloride / n-heptane; tetrahydrofuran / 5 h / -30 - -25 °C / Inert atmosphere
2.2: 10 h / 20 °C
With
sodium hydride; (-)-diisopinocamphenylborane chloride;
In
tetrahydrofuran; n-heptane; mineral oil;