8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione

Base Information

Chemical Name:8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione
CAS No.:126588-04-3
Molecular Formula:C₂₀H₁₈N₂O₅
Molecular Weight:366.373
Hs Code.:

Synonyms:8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione

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Chemical Property of 8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione

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Technology Process of 8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione

There total 1 articles about 8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126588-03-2
(2R,4S)-1-(4-Benzyloxy-5-methoxy-2-nitro-benzoyl)-4-hydroxy-pyrrolidine-2-carboxylic acid ethyl ester

: 126588-04-3
8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione

Guidance literature:: With chromium(VI) oxide; sulfuric acid; tin(ll) chloride; Multistep reaction; 1.) EtOH, 75-80 deg C, 2.) (CH₃)2CO;
DOI:10.1016/S0040-4039(01)93348-9

Reference yield: 75.0%

: 126588-04-3
8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione

: 126588-06-5
8-Benzyloxy-2-chloro-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-5,11-dione

Guidance literature:: With trichlorophosphate; at 80 - 90 ℃; for 1.5h;
DOI:10.1016/S0040-4039(01)93348-9

Reference yield: 71.0%

: 126588-04-3
(S)-8-Benzyloxy-7-methoxy-1,11a-dihydro-10H-benzo[e]pyrrolo[1,2-a][1,4]diazepine-2,5,11-trione

: 132391-66-3
(2S,11aS)-2-hydroxy-8-(benzyloxy)-1,2,3,10,11,11a-hexahydro-7-methoxy-5H-pyrrolo<2,1-c><1,4>benzodiazepine-5,11-dione

Guidance literature:: at 37 ℃; for 72h; baker's yeast (Saccharomyces cerevisiae, Sigma, Type I), 0.1 M phosphate buffer pH 7.4, glucose, aerobic conditions;
DOI:10.1021/jo00006a051