2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:161767-54-0
Molecular Formula:C₂₁H₂₄ClNO₁₂
Molecular Weight:517.874
Hs Code.:

Synonyms:2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Chemical Property of 2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of 2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 3 articles about 2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 161767-53-9
2-bromomethyl-4-nitrophenyl tetra-O-acetyl-β-D-glucopyranoside

: 161767-54-0
2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With tetrabutyl-ammonium chloride; In acetonitrile; for 4h; Heating;
DOI:10.1039/P19950000027

Reference yield:

: 161767-52-8
2-methyl-4-nitrophenyl tetra-O-acetyl-β-D-glucopyranoside

: 161767-54-0
2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / 1,3-dibromo-5,5-dimethylhydantoin, azoisobutyronitrile / benzene / 3.5 h / Heating; Irradiation

2: 64 percent / tetrabutylammonium chloride / acetonitrile / 4 h / Heating

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); tetrabutyl-ammonium chloride; In acetonitrile; benzene;
DOI:10.1039/P19950000027

Reference yield:

: 5346-66-7,32742-28-2,33535-32-9,84380-03-0
2-methylphenyl-(2,3,4,6-tetra-O-acetyl)-β-D-glucopyranoside

: 161767-54-0
2-chloromethyl-4-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 14 percent / nitric acid, trifluoroacetic anhydride / 0.17 h / 0 - 5 °C

2: 56 percent / 1,3-dibromo-5,5-dimethylhydantoin, azoisobutyronitrile / benzene / 3.5 h / Heating; Irradiation

3: 64 percent / tetrabutylammonium chloride / acetonitrile / 4 h / Heating

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; 2,2'-azobis(isobutyronitrile); tetrabutyl-ammonium chloride; nitric acid; trifluoroacetic anhydride; In acetonitrile; benzene;
DOI:10.1039/P19950000027