6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione

Base Information

Chemical Name:6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione
CAS No.:220759-04-6
Molecular Formula:C₃₃H₄₇N₅O₂
Molecular Weight:545.768
Hs Code.:

6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[<i>cd</i>]indene-1,4-dione

Synonyms:6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione

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Chemical Property of 6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione

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Technology Process of 6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione

There total 5 articles about 6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 220759-03-5
[2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]inden-6-yl]-carbamic acid benzyl ester

: 220759-04-6
6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; acetic acid; ethyl acetate; for 3h;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1

Reference yield:

: 220759-00-2
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid

: 220759-04-6
6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) diphenylphosphoryl azide / 1.) PhMe, r.t., 30 min, 2.) PhMe, reflux, 2 h

2: 91 percent / H₂ / Pd/C / ethanol; ethyl acetate; acetic acid / 3 h

With diphenylphosphoranyl azide; hydrogen; palladium on activated charcoal; In ethanol; acetic acid; ethyl acetate;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1

Reference yield:

: 220758-99-6
2a,7b-bis-(4-heptyl-phenyl)-1,4-dioxo-octahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-6-carboxylic acid benzyl ester

: 220759-04-6
6-amino-2a,7b-bis-(4-heptyl-phenyl)-tetrahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-1,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / Pd/C / ethanol / 3 h

2: 1.) diphenylphosphoryl azide / 1.) PhMe, r.t., 30 min, 2.) PhMe, reflux, 2 h

3: 91 percent / H₂ / Pd/C / ethanol; ethyl acetate; acetic acid / 3 h

With diphenylphosphoranyl azide; hydrogen; palladium on activated charcoal; In ethanol; acetic acid; ethyl acetate;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3410::AID-ANIE3410>3.0.CO;2-1