1-(acetyloxy)cyclohexanecarboxaldehyde

Base Information

Chemical Name:1-(acetyloxy)cyclohexanecarboxaldehyde
CAS No.:56037-77-5
Molecular Formula:C₉H₁₄O₃
Molecular Weight:170.208
Hs Code.:

Synonyms:1-(acetyloxy)cyclohexanecarboxaldehyde

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Chemical Property of 1-(acetyloxy)cyclohexanecarboxaldehyde

Chemical Property:

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Technology Process of 1-(acetyloxy)cyclohexanecarboxaldehyde

There total 9 articles about 1-(acetyloxy)cyclohexanecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 32379-37-6
1-Acetoxy-cyclohexylcyanid

: 56037-77-5
1-(acetyloxy)cyclohexanecarboxaldehyde

Guidance literature:: With sulfuric acid; hydrogen; nickel; In ethanol;
DOI:10.1002/ardp.19813140607

Reference yield: 45.0%

: 53282-55-6
(trimethylsiloxymethylidene)cyclohexane

: 56037-77-5
1-(acetyloxy)cyclohexanecarboxaldehyde

Guidance literature:: With lead(IV) acetate; potassium acetate; In acetic acid; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88584-7

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 56037-77-5
1-(acetyloxy)cyclohexanecarboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / K₂CO₃ / 2 h / Heating

2: MCPBA / CH₂Cl₂ / 4 h / Ambient temperature

3: BF₃/ether / CH₂Cl₂

With diethyl ether; boron trifluoride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo00164a014