N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin

Base Information

Chemical Name:N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin
CAS No.:76885-86-4
Molecular Formula:C₃₀H₃₆N₂O₁₂
Molecular Weight:616.622
Hs Code.:

Synonyms:N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin

Suppliers and Price of N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin

Chemical Property:

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Technology Process of N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin

There total 7 articles about N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 76902-48-2
[(2S,4aS,5S,6S,7R,8S,8aR,9aS,10aR)-5-(Benzyloxycarbonyl-methyl-amino)-4a,6,8-trihydroxy-2-hydroxymethyl-4-methoxy-4a,5,6,7,8,8a,9a,10a-octahydro-2H-1,9,10-trioxa-anthracen-7-yl]-methyl-carbamic acid benzyl ester

: 76885-86-4
N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin

Guidance literature:: With hydrogenchloride; In tetrahydrofuran;
DOI:10.1016/0040-4039(80)88067-1

Reference yield:

: C₂₂H₃₂Cl₂N₂O₁₄

: 76885-86-4
N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylformamide

2: 15 percent / HCl(aq.),CH₃CHO / acetonitrile

3: 96 percent / KHCO₃ / acetonitrile / 120 h / 25 °C

4: HCl(aq.) / tetrahydrofuran

With hydrogenchloride; potassium hydrogencarbonate; acetaldehyde; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0040-4039(80)88067-1

Reference yield:

: 64979-02-8
N,N'-<(benzyloxy)carbonyl>actinamine

: 76885-86-4
N,N'-dicarbobenzyloxy-6'-hydroxyspectinomycin

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylformamide

2: 15 percent / HCl(aq.),CH₃CHO / acetonitrile

3: 96 percent / KHCO₃ / acetonitrile / 120 h / 25 °C

4: HCl(aq.) / tetrahydrofuran

With hydrogenchloride; potassium hydrogencarbonate; acetaldehyde; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0040-4039(80)88067-1