2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester

Base Information

Chemical Name:2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester
CAS No.:496863-31-1
Molecular Formula:C₂₂H₃₁NO₄S₂
Molecular Weight:437.624
Hs Code.:

Synonyms:2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester

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Technology Process of 2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester

There total 1 articles about 2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 438044-55-4
2,2-dimethylpropanoic acid 1-[(methylcarbamoyl)methyl]-2,2-bis(methylsulfanyl)ethyl ester

: 3-phenylbut-3-enoyl chloride

: 496863-31-1
2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester

Guidance literature:: With molecular sieve; In dichloromethane; at 20 ℃;
DOI:10.3987/COM-02-S(M)12

Reference yield: 64.0%

: 496863-31-1
2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester

: 496863-32-2
3-phenyl-but-3-enoic acid methyl-(5-methylsulfanyl-furan-2-yl)-amide

Guidance literature:: With dimethyl(methylthio)sulfonium tetrafluoroborate; In acetonitrile; at -40 ℃; for 1h;
DOI:10.3987/COM-02-S(M)12

Reference yield:

: 496863-31-1
2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-[methyl(3-phenylbut-3-enoyl)amino]-3-oxopropyl ester

: 496863-35-5
1-methyl-6-(methylsulfanyl)-3a-phenyl-2,3,3a,4-tetrahydroindol-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / dimethyl(methylthio)sulfonium tetrafluoroborate / acetonitrile / 1 h / -40 °C

2: 61 percent / benzene / 8 h / Heating

3: 65 percent / cerium chloride heptahydrate; sodium borohydride / methanol / 3 h / 0 °C

4: 88 percent / triethylamine; mesyl chloride / CH₂Cl₂ / 20 °C

With sodium tetrahydroborate; cerium(III) chloride; dimethyl(methylthio)sulfonium tetrafluoroborate; methanesulfonyl chloride; triethylamine; In methanol; dichloromethane; acetonitrile; benzene; 2: intramolecular Diels-Alder reaction;
DOI:10.3987/COM-02-S(M)12