C₃₂H₂₁Cl

Base Information

Chemical Name:C₃₂H₂₁Cl
CAS No.:1329425-10-6
Molecular Formula:C₃₂H₂₁Cl
Molecular Weight:440.972
Hs Code.:

Synonyms:C₃₂H₂₁Cl

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Chemical Property of C₃₂H₂₁Cl

Chemical Property:

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Technology Process of C₃₂H₂₁Cl

There total 7 articles about C₃₂H₂₁Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1329425-08-2
C₂₄H₁₂BrCl

: 100379-00-8
2,6-dimethylbenzene boronic acid

: 1329425-10-6
C₃₂H₂₁Cl

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 90 ℃; for 6h;

Reference yield:

: 92866-01-8
2-bromo-3-fluorantheneamine

: 1329425-10-6
C₃₂H₂₁Cl

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / ethanol / 0.5 h / 0 °C

1.2: 1 h / 0 °C

1.3: 5 h / Reflux

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 4 h / 90 °C

3.1: potassium tert-butylate / diethyl ether; tetrahydrofuran / 1 h / 20 °C

3.2: 5 h / 20 °C

4.1: methanesulfonic acid / dichloromethane / 17 h / 20 °C

5.1: bromine / dichloromethane; chloroform / 18.5 h / 0 - 20 °C

6.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 6 h / 90 °C

With methanesulfonic acid; sulfuric acid; potassium tert-butylate; bromine; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; chloroform; water; toluene;

Reference yield:

: 1329425-07-1
C₂₄H₁₃Cl

: 1329425-10-6
C₃₂H₂₁Cl

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / dichloromethane; chloroform / 18.5 h / 0 - 20 °C

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 6 h / 90 °C

With bromine; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; chloroform; water; toluene;