C₄₅H₃₄N₈OS

Base Information

• Chemical Name: C₄₅H₃₄N₈OS
• CAS No.: 1029889-26-6
• Molecular Formula: C₄₅H₃₄N₈OS
• Molecular Weight: 734.884
• Mol file: 1029889-26-6.mol

Synonyms:C₄₅H₃₄N₈OS

Chemical Property of C₄₅H₃₄N₈OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₃₄N₈OS

There total 7 articles about C₄₅H₃₄N₈OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole (133051-88-4) + 5-(5-Methyl-isoxazol-3-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol (114461-19-7) → C45H34N8OS (1029889-26-6)

Guidance literature:

5-(5-Methyl-isoxazol-3-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol; With potassium carbonate; In acetone; for 2h; Heating;

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole; In acetone; Further stages.; Heating;

DOI:10.1002/jccs.200700115

Reference yield:

5-methylisoxazole-3-carboxylic acid hydrazide (62438-03-3) → C45H34N8OS (1029889-26-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ethanol

2.1: aq. K₂CO₃

3.1: K₂CO₃ / acetone / 2 h / Heating

3.2: 83 percent / acetone / Heating

With potassium carbonate; In ethanol; acetone;

DOI:10.1002/jccs.200700115

Reference yield:

2-Cyano-4'-methylbiphenyl (114772-53-1) → C45H34N8OS (1029889-26-6)

Guidance literature:

Multi-step reaction with 4 steps

1.1: zinc chloride; sodium azide / dimethylformamide / 36 h / Heating

1.2: 96 percent / aq. HCl / dimethylformamide / 1 h / cooling

2.1: 91 percent / aq. NaOH / toluene / 3 h / 20 °C

3.1: 92 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl₄ / 8 h / Heating

4.1: K₂CO₃ / acetone / 2 h / Heating

4.2: 83 percent / acetone / Heating

With sodium hydroxide; N-Bromosuccinimide; sodium azide; potassium carbonate; zinc(II) chloride; dibenzoyl peroxide; In tetrachloromethane; N,N-dimethyl-formamide; acetone; toluene;

DOI:10.1002/jccs.200700115

upstream raw materials:

N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

5-(5-Methyl-isoxazol-3-yl)-4-phenyl-4H-[1,2,4]triazole-3-thiol

5-methylisoxazole-3-carboxylic acid hydrazide

2-Cyano-4'-methylbiphenyl