C₆₄H₇₆O₁₂

Base Information

Chemical Name:C₆₄H₇₆O₁₂
CAS No.:465518-96-1
Molecular Formula:C₆₄H₇₆O₁₂
Molecular Weight:1037.3
Hs Code.:

C<sub>64</sub>H<sub>76</sub>O<sub>12</sub>

Synonyms:C₆₄H₇₆O₁₂

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Chemical Property of C₆₄H₇₆O₁₂

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Technology Process of C₆₄H₇₆O₁₂

There total 8 articles about C₆₄H₇₆O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 465518-95-0
C₆₄H₇₈O₁₃

: 465518-96-1
C₆₄H₇₆O₁₂

Guidance literature:: C₆₄H₇₈O₁₃; With ortho-nitrophenyl selenocyanate; tributylphosphine; In tetrahydrofuran; for 30h;

With dihydrogen peroxide; In tetrahydrofuran; at 0 - 20 ℃; Further stages.;
DOI:10.1021/ja027346p

Reference yield:

: (3R,9R)-3,9-Bis-((2R,3R,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-carboxyoxy-tetrahydro-pyran-2-yloxy)-decanoic acid isopropyl ester

: 465518-96-1
C₆₄H₇₆O₁₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

2.1: tri-n-butylphosphine; o-nitrophenyl selenocyanate / tetrahydrofuran / 30 h

2.2: 90 percent / aq. H₂O₂ / tetrahydrofuran / 0 - 20 °C

With lithium aluminium tetrahydride; ortho-nitrophenyl selenocyanate; tributylphosphine; In tetrahydrofuran;
DOI:10.1021/ja027346p

Reference yield:

: 932-56-9
2-methyl-cycloheptanone

: 465518-96-1
C₆₄H₇₆O₁₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 74 percent / aq. mCPBA / CH₂Cl₂ / 20 h / Heating

2.1: porcine liver esteraze; NaOH / aq. phosphate buffer / pH 7.2

3.1: carbonyl diimidazole / tetrahydrofuran / 4 h / 0 °C

3.2: 74 percent / tetrahydrofuran / cooling

4.1: 99 percent / [((R)-BINAP)RuCl₂]2*NEt₃; H₂ / methanol; tetrahydrofuran / 15 h / 65 °C / 15001.5 Torr

5.1: molecular sieves 4 Angstroem / CH₂Cl₂ / 0.5 h / 20 °C

5.2: 82 percent / TMSOTf / CH₂Cl₂ / 2.5 h / -78 °C

6.1: 82 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

7.1: tri-n-butylphosphine; o-nitrophenyl selenocyanate / tetrahydrofuran / 30 h

7.2: 90 percent / aq. H₂O₂ / tetrahydrofuran / 0 - 20 °C

With sodium hydroxide; lithium aluminium tetrahydride; ortho-nitrophenyl selenocyanate; tributylphosphine; [((R)-Binap)-RuCl₂]2; 4 A molecular sieve; porcine liver esteraze; hydrogen; 3-chloro-benzenecarboperoxoic acid; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; phosphate buffer; dichloromethane;
DOI:10.1021/ja027346p