methyl 2,3,6-tri-O-benzyl-4-trimethylsilylethynyl-α-D-galactopyranoside

Base Information

Chemical Name:methyl 2,3,6-tri-O-benzyl-4-trimethylsilylethynyl-α-D-galactopyranoside
CAS No.:127924-43-0
Molecular Formula:C₃₃H₄₀O₆Si
Molecular Weight:560.763
Hs Code.:

Synonyms:methyl 2,3,6-tri-O-benzyl-4-trimethylsilylethynyl-α-D-galactopyranoside

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Chemical Property of methyl 2,3,6-tri-O-benzyl-4-trimethylsilylethynyl-α-D-galactopyranoside

Chemical Property:

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Technology Process of methyl 2,3,6-tri-O-benzyl-4-trimethylsilylethynyl-α-D-galactopyranoside

There total 9 articles about methyl 2,3,6-tri-O-benzyl-4-trimethylsilylethynyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127924-40-7
methyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1066-54-2
trimethylsilylacetylene

: 127924-42-9,127924-43-0,127924-44-1,127964-43-6
(2R,4R,5R,6R)-4,5-Bis-benzyloxy-2-benzyloxymethyl-6-methoxy-3-trimethylsilanylethynyl-tetrahydro-pyran-3-ol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(00)76178-8

Reference yield:

: 98807-61-5
1-O-methyl-2,3,6-tri-O-benzyl-4-keto-α-D-glucopyranoside

: 1066-54-2
trimethylsilylacetylene

: 127924-42-9,127924-43-0,127924-44-1,127964-43-6
(2R,4R,5R,6S)-4,5-Bis-benzyloxy-2-benzyloxymethyl-6-methoxy-3-trimethylsilanylethynyl-tetrahydro-pyran-3-ol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(00)76178-8

Reference yield:

: 98807-61-5
1-O-methyl-2,3,6-tri-O-benzyl-4-keto-α-D-glucopyranoside

: 1066-54-2
trimethylsilylacetylene

: 127924-43-0
methyl 2,3,6-tri-O-benzyl-4-trimethylsilylethynyl-α-D-galactopyranoside

: 127924-44-1
methyl 2,3,6-tri-O-benzyl-4-trimethylsilylethynyl-α-D-glucopyranoside

Guidance literature:: trimethylsilylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

1-O-methyl-2,3,6-tri-O-benzyl-4-keto-α-D-glucopyranoside; In tetrahydrofuran; hexane; at -78 ℃; for 3h; optical yield given as %de; Inert atmosphere;
DOI:10.1055/s-0029-1217403