N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide

Base Information

Chemical Name:N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide
CAS No.:1620644-82-7
Molecular Formula:C₃₀H₃₀N₂O₄
Molecular Weight:482.579
Hs Code.:

Synonyms:N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide

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Chemical Property of N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide

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Technology Process of N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide

There total 5 articles about N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53133-41-8
4-(benzylamino) but-3-en-2-one

: 1620646-05-0
3,4-dimethoxy-N-(4-oxobut-2-enyl)-N-phenylbenzamide

: 1620644-82-7
N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide

Guidance literature:: With magnesium(II) perchlorate; magnesium sulfate; In dichloromethane; at 20 ℃;

Reference yield:

: 93-07-2
Veratric acid

: 1620644-82-7
N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylaluminum / toluene / 0.5 h / 20 °C

1.2: 18 h / 80 °C

2.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 22 h / 50 °C / Inert atmosphere

3.1: magnesium(II) perchlorate; magnesium sulfate / dichloromethane / 20 °C

With Hoveyda-Grubbs catalyst second generation; magnesium(II) perchlorate; trimethylaluminum; magnesium sulfate; In dichloromethane; toluene;

Reference yield:

: 100-46-9
benzylamine

: 1620644-82-7
N-[(3-acetyl-1-benzyl-1,4-dihydropyridin-4-yl)methyl]-3,4-dimethoxy-N-phenylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform / 20 °C

2: magnesium(II) perchlorate; magnesium sulfate / dichloromethane / 20 °C

With magnesium(II) perchlorate; magnesium sulfate; In dichloromethane; chloroform;