10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

Base Information

Chemical Name:10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one
CAS No.:130564-08-8
Molecular Formula:C₂₅H₃₁N₃O
Molecular Weight:389.541
Hs Code.:

Synonyms:10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

Suppliers and Price of 10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

There total 2 articles about 10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 130564-05-5
3,8,10,10,10a-pentamethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

: 100-10-7
4-dimethylamino-benzaldehyde

: 130564-08-8
10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

Guidance literature:: With acetic anhydride; In acetic acid; at 95 ℃;
DOI:10.1007/BF00487427

Reference yield:

: 107945-85-7
2,3,3,5-tetramethyl-3H-indole hydrochloride

: 130564-08-8
10a-(4-dimethylaminostyryl)-3,8,10,10-tetramethyl-1,2,3,4,10,10a-hexahydropyrimido<1,2-a>indol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / acetic acid / 100 °C

2: 65 percent / Ac₂O / acetic acid / 95 °C

With acetic anhydride; In acetic acid;
DOI:10.1007/BF00487427