benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

Base Information

• Chemical Name: benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside
• CAS No.: 85230-49-5
• Molecular Formula: C₂₉H₄₀N₂O₁₄
• Molecular Weight: 640.642

Synonyms:benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

Chemical Property of benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

Chemical Property:

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Technology Process of benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

There total 2 articles about benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.6%

benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside (29709-55-5,85054-26-8,85280-48-4) → benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside (85230-49-5)

Guidance literature:

With acetic acid; In water; at 85 ℃; for 1.5h;

DOI:10.1016/0008-6215(83)88219-6

Reference yield:

→ Benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-β-D-glucopyranosid (85230-49-5)

Guidance literature:

9, 50percentig. wssr. Essigsaeure;

DOI:10.1016/S0008-6215(00)80289-X

Reference yield:

2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)-<2,1-d>-2-oxazoline + benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside (85230-49-5) → C43H59N3O22 (85230-53-1)

Guidance literature:

With toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 70 ℃; for 36h;

DOI:10.1016/0008-6215(83)88219-6

upstream raw materials:

benzyl 2-acetamido-3-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

Downstream raw materials:

C₄₃H₅₉N₃O₂₂

benzyl 2-acetamido-3-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2,6-dideoxy-6-fluoro-α-D-galactopyranoside

benzyl 2-acetamido-3,6-di-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-α-D-galactopyranoside

benzyl 2-acetamido-3,6-di-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-O-acetyl-2-deoxy-α-D-galactopyranoside

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