16,17-seco-3-methoxyestra-1,3,5⁽¹⁰⁾trien-17-al oxime 4'-nitrobenzyl ether

Base Information

Chemical Name:16,17-seco-3-methoxyestra-1,3,5⁽¹⁰⁾trien-17-al oxime 4'-nitrobenzyl ether
CAS No.:1187251-85-9
Molecular Formula:C₂₇H₃₄N₂O₄
Molecular Weight:450.578
Hs Code.:

16,17-seco-3-methoxyestra-1,3,5<sup>(10)</sup>trien-17-al oxime 4'-nitrobenzyl ether

Synonyms:16,17-seco-3-methoxyestra-1,3,5⁽¹⁰⁾trien-17-al oxime 4'-nitrobenzyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 16,17-seco-3-methoxyestra-1,3,5⁽¹⁰⁾trien-17-al oxime 4'-nitrobenzyl ether

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Technology Process of 16,17-seco-3-methoxyestra-1,3,5⁽¹⁰⁾trien-17-al oxime 4'-nitrobenzyl ether

There total 1 articles about 16,17-seco-3-methoxyestra-1,3,5⁽¹⁰⁾trien-17-al oxime 4'-nitrobenzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2086-26-2
O-(p-nitrobenzyl)hydroxylamine hydrochloride

: 221454-64-4
3-methoxyestra-16,17-seco-1,3,5⁽¹⁰⁾-trien-17-al

: 1187251-85-9
16,17-seco-3-methoxyestra-1,3,5⁽¹⁰⁾trien-17-al oxime 4'-nitrobenzyl ether

Guidance literature:: With sodium acetate; In isopropyl alcohol; for 8h; Reflux;
DOI:10.1002/ejoc.200900301

Reference yield: 78.0%

: 1187251-85-9
16,17-seco-3-methoxyestra-1,3,5⁽¹⁰⁾trien-17-al oxime 4'-nitrobenzyl ether

: 1187251-88-2
C₂₇H₃₄N₂O₄

Guidance literature:: With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.200900301