N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate

Base Information

Chemical Name:N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate
CAS No.:1334709-95-3
Molecular Formula:C₁₀₈H₁₁₆Cl₃N₇O₂₉SSi
Molecular Weight:2142.65
Hs Code.:

N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate

Synonyms:N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate

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Chemical Property of N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate

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Technology Process of N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate

There total 1 articles about N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₉₄H₁₀₄Cl₃N₇O₂₉SSi

: 908094-04-2
phenyldiazomethane

: 1334709-95-3
N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate

Guidance literature:: In diethyl ether; dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/chem.201101108

Reference yield: 85.0%

: 1334709-95-3
N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate

: 1334709-96-4
N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate-(1->4)-6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-benzyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyluronate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/chem.201101108