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thallium phenylcyanamidate

Base Information
  • Chemical Name:thallium phenylcyanamidate
  • CAS No.:35341-02-7
  • Molecular Formula:C7H5N2*Tl
  • Molecular Weight:321.513
  • Hs Code.:
thallium phenylcyanamidate

Synonyms:thallium phenylcyanamidate

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Chemical Property of thallium phenylcyanamidate
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Technology Process of thallium phenylcyanamidate

There total 1 articles about thallium phenylcyanamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In water; acetone; mixing equimolar amt. of TlOAc with neutralized cyanamide (in 50% aq. acetone);
DOI:10.1016/S0020-1693(00)88908-2
Guidance literature:
In dichloromethane; addn. of thallium compd. to CH2C2 soln. of porphyrin deriv. under N2, stirring for 1 h; filtration, evapn., recrystn. by addn. of n-hexane to CH2Cl2 soln., isolation of crystals, elem. anal.;
DOI:10.1016/j.ica.2008.06.029
Guidance literature:
In water; byproducts: TlCl; aq. soln. of thallium salt was added to aq. soln. of praseodymium complex, stirred for 3 h; filtered, washed with hot water, extd. with CH2Cl2, evapd. in vac., crystd. from CH2Cl2/Et2O, dried in vac. over P2O5 for several hours, elem. anal.;
DOI:10.1016/j.ica.2009.04.040
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