3-bromo[methoxy[(1-[t-butyldiphenylsilyloxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]benzene

Base Information

Chemical Name:3-bromo[methoxy[(1-[t-butyldiphenylsilyloxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]benzene
CAS No.:1239339-92-4
Molecular Formula:C₃₂H₄₃BrO₃Si₂
Molecular Weight:611.767
Hs Code.:

Synonyms:3-bromo[methoxy[(1-[t-butyldiphenylsilyloxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]benzene

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Chemical Property of 3-bromo[methoxy[(1-[t-butyldiphenylsilyloxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]benzene

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Technology Process of 3-bromo[methoxy[(1-[t-butyldiphenylsilyloxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]benzene

There total 1 articles about 3-bromo[methoxy[(1-[t-butyldiphenylsilyloxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1239339-88-8
C₈H₈BrClO

: 1239339-82-2
1-(t-butyldiphenylsilyloxy)-3-((trimethylsilyl)methyl)but-3-en-2-ol

: 1239339-92-4
3-bromo[methoxy[(1-[t-butyldiphenylsilyloxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]benzene

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0cc00467g

Reference yield:

: 1239339-92-4
3-bromo[methoxy[(1-[t-butyldiphenylsilyloxy]methyl-2-[(trimethylsilyl)methyl]prop-2-en-1-yl)oxy]methyl]benzene

: 5-(3-bromophenyl)-2-((t-butyldiphenylsilyloxy)methyl)-3-methylenetetrahydrofuran

: 5-(3-bromophenyl)-2-((t-butyldiphenylsilyloxy)methyl)-3-methylenetetrahydrofuran

Guidance literature:: With trimethylsilyl bis(trifluoromethanesulfonyl)imide; In dichloromethane; at -78 ℃; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c0cc00467g