ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate

Base Information

Chemical Name:ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate
CAS No.:1025722-94-4
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

Synonyms:ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate

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Chemical Property of ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate

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Technology Process of ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate

There total 1 articles about ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1025722-65-9
ethyl (4S,2Z)-4-[N-(tert-butoxycarbonyl)amino]-5-phenyl-3-[(trifluoromethanesulfonyl)oxy]pent-2-enoate

: 98-80-6
phenylboronic acid

: 1025722-94-4
ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate

Guidance literature:: With potassium phosphate; potassium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 85 ℃; for 12h;
DOI:10.1021/jo702318d

Reference yield: 63.0%

: 1025722-94-4
ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate

: 79-22-1
methyl chloroformate

: 1025723-06-1
methyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enyl carbonate

Guidance literature:: ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3,5-diphenylpent-2-enoate; With boron trifluoride diethyl etherate; diisobutylaluminium hydride; In dichloromethane; toluene; at 0 ℃; for 0.5h;

methyl chloroformate; With pyridine; dmap; In dichloromethane; at 0 ℃; for 1h; Further stages.;
DOI:10.1021/jo702318d