N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide

Base Information

Chemical Name:N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide
CAS No.:253877-85-9
Molecular Formula:C₄₂H₅₄N₄O₄
Molecular Weight:678.915
Hs Code.:

Synonyms:N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide

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Chemical Property of N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide

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Technology Process of N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide

There total 5 articles about N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Biphenyl-4,4'-dicarboxylic acid bis-[(6-{[1-(2-methoxy-phenyl)-meth-(E)-ylidene]-amino}-hexyl)-amide]

: 253877-85-9
N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 18h;
DOI:10.1021/jm991110n

Reference yield:

: 787-70-2
4,4'-diphenic acid

: 253877-85-9
N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N / dioxane / 0.5 h / 5 °C

2: dioxane / 20 °C

3: 100 percent / HBr; CF₃CO₂H / acetic acid / 1 °C

4: 3 Angstroem sieves / methanol / 0.5 h / 20 °C

5: NaBH₄ / methanol / 18 h / 20 °C

With sodium tetrahydroborate; 3 A molecular sieve; hydrogen bromide; triethylamine; trifluoroacetic acid; In 1,4-dioxane; methanol; acetic acid; 1: Acetoxylation / 2: Condensation / 3: Hydrolysis / 4: Condensation / 5: Reduction;
DOI:10.1021/jm991110n

Reference yield:

: C₂₀H₁₈O₈

: 253877-85-9
N,N'-di{6-[(2-methoxybenzyl)amino]hexyl}-1,1'-biphenyl-4,4'-diyldiamide

Guidance literature:: Multi-step reaction with 4 steps

1: dioxane / 20 °C

2: 100 percent / HBr; CF₃CO₂H / acetic acid / 1 °C

3: 3 Angstroem sieves / methanol / 0.5 h / 20 °C

4: NaBH₄ / methanol / 18 h / 20 °C

With sodium tetrahydroborate; 3 A molecular sieve; hydrogen bromide; trifluoroacetic acid; In 1,4-dioxane; methanol; acetic acid; 1: Condensation / 2: Hydrolysis / 3: Condensation / 4: Reduction;
DOI:10.1021/jm991110n