[tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester

Base Information

Chemical Name:[tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester
CAS No.:762288-82-4
Molecular Formula:C₂₅H₄₁N₃O₉S
Molecular Weight:559.681
Hs Code.:

[<i>tert</i>-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid <i>tert</i>-butyl ester

Synonyms:[tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester

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Chemical Property of [tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester

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Technology Process of [tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester

There total 1 articles about [tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 138-41-0
4-(aminosulfonyl)-benzoic acid

: 225115-71-9
tert-butyl 2-(2-(2-(2-aminoethoxy)ethoxy)ethyl)((tert-butyloxycarbonyl)methylamino)acetate

: 762288-82-4
[tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/ja047557p

Reference yield: 99.0%

: 762288-82-4
[tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester

: [carboxymethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 5h;
DOI:10.1021/ja047271k

Reference yield: 91.0%

: copper(II) choride dihydrate

: 762288-82-4
[tert-butoxycarbonylmethyl-(2-{2-[2-(4-sulfamoyl-benzoylamino)-ethoxy]-ethoxy}-ethyl)-amino]-acetic acid tert-butyl ester

: Cu⁽²⁺⁾*NH₂SO₂C₆H₄CONHC₂H₄OC₂H₄OC₂H₄N(CH₂CO₂)2^(2-)*H₂O=Cu(NH₂SO₂C₆H₄CONHC₆H₁₂O₂N(CH₂CO₂)2)*H₂O

Guidance literature:: With sodium hydrogencarbonate; In methanol; water; aq. soln. of satd. NaHCO3 was added to a soln. of acid sulfonamide in methanol, solid CuCl2*2H2O was added with stirring, the mixt. was stired for 30 min at room temp.; evapd. to dryness under reduced pressure, the residue was dissolved in min water, methanol was added, ppt. was filtered, dissolved in water, pptd. by ethanol, filtered, dried under vac.; elem. anal.;
DOI:10.1021/ja047557p