cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate

Base Information

Chemical Name:cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate
CAS No.:1449397-08-3
Molecular Formula:C₃₂H₃₆ClF₃N₈O₄
Molecular Weight:689.137
Hs Code.:

cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate

Synonyms:cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate

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Chemical Property of cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate

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Technology Process of cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate

There total 8 articles about cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449410-58-5
C₃₄H₃₃ClF₃N₇O₅

: 7252-53-1
(aminomethyl)cyclopropane hydrochloride

: 1449397-08-3
cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 4h;

Reference yield:

: 1360828-40-5
tert-butyl 4-((4-((1-(4-chlorophenyl)cyclopropyl)amino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl)amino)benzoate

: 1449397-08-3
cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / 1,4-dioxane / 4 h

2: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 16 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

4: tetrahydrofuran / 16 h / 20 °C

5: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 4 h / 20 °C

With hydrogenchloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 185677-00-3
2,4-dichloro-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine

: 1449397-08-3
cyclopropylmethyl 2-(3-(4-{[4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino}benzamido)-2,2-dimethylpropylamino)-2-oxoacetate

Guidance literature:: Multi-step reaction with 7 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h

2: tetrahydrofuran / 5 h / 80 °C

3: hydrogenchloride / 1,4-dioxane / 4 h

4: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 16 h / 20 °C

5: trifluoroacetic acid / dichloromethane / 16 h / 20 °C

6: tetrahydrofuran / 16 h / 20 °C

7: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 4 h / 20 °C

With hydrogenchloride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;